PDF (Volume 2)12MbAbstractThree series of alkoxy substituted tolans p X C(_6)H(_4) CC C(_6)H(_4) p OC(_n)H(_2n+1) [X = H (series 1) steroids, CH(_3) (series 2), OCH(_3) (series 3)] with varying chain length were synthesized by Pd/Cu catalysed Sonogashira cross coupling reactions of terminal alkynes and iodoarenes, crystal structures and phase behavior of three series of tolans. Twenty eight of the tolans were structurally characterised by single crystal X ray diffraction. Their phase behavior was characterised by tplm; only the tolans in series 3 show liquid crystalline phases.

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